1H and 13C NMR spectral assignments of pyridinium salts linked to a N-9 or N-3 adenine moiety

Belén Rubio-Ruiz; Ana Conejo-García; Miguel A Gallo; Antonio Espinosa; Antonio Entrena

doi:10.1002/mrc.3817

1H and 13C NMR spectral assignments of pyridinium salts linked to a N-9 or N-3 adenine moiety

Belén Rubio-Ruiz, Ana Conejo-García, Miguel A Gallo, Antonio Espinosa, Antonio Entrena

Research output: Contribution to journal › Article › peer-review

Abstract / Description of output

(1)H and (13)C NMR spectral data of 13 new compounds containing a 4-(dimethylamino)- or 4-(pyrrolidin-1-yl)pyridinium moiety linked to the N-9 or N-3 nitrogen atom of an adenine moiety were assigned. 1D and 2D NMR experiments (DEPT, HSQC and HMBC) allowed the unequivocal identification of N-9 and N-3 isomers.

Original language	English
Pages (from-to)	466-9
Number of pages	4
Journal	Magnetic Resonance in Chemistry
Volume	50
Issue number	6
DOIs	https://doi.org/10.1002/mrc.3817
Publication status	Published - Jun 2012

Keywords / Materials (for Non-textual outputs)

Adenine
Carbon Isotopes
Choline Kinase
Enzyme Inhibitors
Isomerism
Molecular Structure
Nitrogen
Nuclear Magnetic Resonance, Biomolecular
Protons
Pyridinium Compounds

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title = "1H and 13C NMR spectral assignments of pyridinium salts linked to a N-9 or N-3 adenine moiety",

abstract = "(1)H and (13)C NMR spectral data of 13 new compounds containing a 4-(dimethylamino)- or 4-(pyrrolidin-1-yl)pyridinium moiety linked to the N-9 or N-3 nitrogen atom of an adenine moiety were assigned. 1D and 2D NMR experiments (DEPT, HSQC and HMBC) allowed the unequivocal identification of N-9 and N-3 isomers.",

keywords = "Adenine, Carbon Isotopes, Choline Kinase, Enzyme Inhibitors, Isomerism, Molecular Structure, Nitrogen, Nuclear Magnetic Resonance, Biomolecular, Protons, Pyridinium Compounds",

author = "Bel{\'e}n Rubio-Ruiz and Ana Conejo-Garc{\'i}a and Gallo, {Miguel A} and Antonio Espinosa and Antonio Entrena",

note = "Copyright {\textcopyright} 2012 John Wiley & Sons, Ltd.",

year = "2012",

month = jun,

doi = "10.1002/mrc.3817",

language = "English",

volume = "50",

pages = "466--9",

journal = "Magnetic Resonance in Chemistry",

issn = "0749-1581",

publisher = "Wiley",

number = "6",

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TY - JOUR

T1 - 1H and 13C NMR spectral assignments of pyridinium salts linked to a N-9 or N-3 adenine moiety

AU - Rubio-Ruiz, Belén

AU - Conejo-García, Ana

AU - Gallo, Miguel A

AU - Espinosa, Antonio

AU - Entrena, Antonio

PY - 2012/6

Y1 - 2012/6

N2 - (1)H and (13)C NMR spectral data of 13 new compounds containing a 4-(dimethylamino)- or 4-(pyrrolidin-1-yl)pyridinium moiety linked to the N-9 or N-3 nitrogen atom of an adenine moiety were assigned. 1D and 2D NMR experiments (DEPT, HSQC and HMBC) allowed the unequivocal identification of N-9 and N-3 isomers.

AB - (1)H and (13)C NMR spectral data of 13 new compounds containing a 4-(dimethylamino)- or 4-(pyrrolidin-1-yl)pyridinium moiety linked to the N-9 or N-3 nitrogen atom of an adenine moiety were assigned. 1D and 2D NMR experiments (DEPT, HSQC and HMBC) allowed the unequivocal identification of N-9 and N-3 isomers.

KW - Adenine

KW - Carbon Isotopes

KW - Choline Kinase

KW - Enzyme Inhibitors

KW - Isomerism

KW - Molecular Structure

KW - Nitrogen

KW - Nuclear Magnetic Resonance, Biomolecular

KW - Protons

KW - Pyridinium Compounds

U2 - 10.1002/mrc.3817

DO - 10.1002/mrc.3817

M3 - Article

C2 - 22528078

SN - 0749-1581

VL - 50

SP - 466

EP - 469

JO - Magnetic Resonance in Chemistry

JF - Magnetic Resonance in Chemistry

IS - 6

ER -

1H and 13C NMR spectral assignments of pyridinium salts linked to a N-9 or N-3 adenine moiety

Abstract / Description of output

Keywords / Materials (for Non-textual outputs)

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