Rapid Estimation of T1 for Quantitative NMR

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Quantitative NMR spectroscopy (qNMR) is an essential tool in organic chemistry, with applications including reaction monitoring, mechanistic analysis, and purity determination. Establishing the correct acquisition rate for consecutive qNMR scans requires knowledge of the longitudinal relaxation time constants (T1) for all of the nuclei being monitored. We report a simple method that is about 10-fold faster than the conventional inversion recovery technique for the estimation of T1.
Original languageEnglish
Pages (from-to)9023–9029
JournalJournal of Organic Chemistry
Issue number13
Early online date22 Jun 2021
Publication statusE-pub ahead of print - 22 Jun 2021


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