Rotating tomography Paris-Edinburgh cell: a novel portable press for micro-tomographic 4-D imaging at extreme pressure/temperature/stress conditions

J. Philippe; Y. Le Godec; M. Mezouar; M. Berg; G. Bromiley; F. Bergame; J. P. Perrillat; M. Alvarez-Murga; M. Morand; Robert Atwood; A. King; S. Regnier

doi:10.1080/08957959.2016.1221951

Rotating tomography Paris-Edinburgh cell: a novel portable press for micro-tomographic 4-D imaging at extreme pressure/temperature/stress conditions

J. Philippe, Y. Le Godec, M. Mezouar, M. Berg, G. Bromiley, F. Bergame, J. P. Perrillat, M. Alvarez-Murga, M. Morand, Robert Atwood, A. King, S. Regnier

Research output: Contribution to journal › Article › peer-review

Abstract / Description of output

This paper presents details of instrumental development to extend synchrotron X-ray microtomography techniques to in situ studies under static compression (high pressure), shear stress or the both conditions at simultaneous high temperatures. To achieve this, a new rotating tomography Paris-Edinburgh cell has been developed. This ultra-compact portable device easily and successfully adapted to various multi-modal synchrotron experimental set-up at ESRF, SOLEIL and DIAMOND is explained in detail. An in-depth description of proof of concept first experiments performed on a high resolution imaging beamline is then given, which illustrate the efficiency of the set-up and the data quality that can be obtained.

Original language	English
Pages (from-to)	512-532
Number of pages	21
Journal	High Pressure Research
Volume	36
Issue number	4
Early online date	6 Sept 2016
DOIs	https://doi.org/10.1080/08957959.2016.1221951
Publication status	Published - 2016

Keywords / Materials (for Non-textual outputs)

High pressure
high temperature
tomography
stress
synchrotron
NEUTRON POWDER DIFFRACTION
IN-SITU
COMPUTED-TOMOGRAPHY
DEFORMATION
TEMPERATURE
APPARATUS
GPA
MICROTOMOGRAPHY
DEVICE

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10.1080/08957959.2016.1221951Licence: Creative Commons: Attribution (CC-BY)

26646262. PFV. Rotating tomography Paris Edinburgh cell a novel portable press for micro tomographic 4 D imaging at extreme pressure temperature stress conditions
© 2016 The Author(s). Published by Informa UK Limited, trading as Taylor & Francis Group. This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Final published version, 4.05 MBLicence: Creative Commons: Attribution (CC-BY)

http://www.tandfonline.com/doi/full/10.1080/08957959.2016.1221951?scroll=top&needAccess=trueLicence: Creative Commons: Attribution (CC-BY)

In-Situ X-ray tomographic imaging under extreme conditions: a proof of concept study
Bromiley, G. & Butler, I.
NERC
1/04/11 → 31/12/12
Project: Research

Electron Probe Microanalysis Facility (EPMA)
Chris Hayward (Manager)
School of Geosciences
Facility/equipment: Facility
Micro CT Scanner (EXP)
Ian Butler (Manager)
School of Geosciences
Facility/equipment: Facility
Scanning Electron Microscope Facility (SEM)
Nicola Cayzer (Manager)
School of Geosciences
Facility/equipment: Facility

Cite this

Philippe, J., Le Godec, Y., Mezouar, M., Berg, M., Bromiley, G., Bergame, F., Perrillat, J. P., Alvarez-Murga, M., Morand, M., Atwood, R., King, A., & Regnier, S. (2016). Rotating tomography Paris-Edinburgh cell: a novel portable press for micro-tomographic 4-D imaging at extreme pressure/temperature/stress conditions. High Pressure Research, 36(4), 512-532. https://doi.org/10.1080/08957959.2016.1221951

@article{f919474342a74872b362b517f6f3749c,

title = "Rotating tomography Paris-Edinburgh cell: a novel portable press for micro-tomographic 4-D imaging at extreme pressure/temperature/stress conditions",

abstract = "This paper presents details of instrumental development to extend synchrotron X-ray microtomography techniques to in situ studies under static compression (high pressure), shear stress or the both conditions at simultaneous high temperatures. To achieve this, a new rotating tomography Paris-Edinburgh cell has been developed. This ultra-compact portable device easily and successfully adapted to various multi-modal synchrotron experimental set-up at ESRF, SOLEIL and DIAMOND is explained in detail. An in-depth description of proof of concept first experiments performed on a high resolution imaging beamline is then given, which illustrate the efficiency of the set-up and the data quality that can be obtained.",

keywords = "High pressure, high temperature, tomography, stress, synchrotron, NEUTRON POWDER DIFFRACTION, IN-SITU, COMPUTED-TOMOGRAPHY, DEFORMATION, TEMPERATURE, APPARATUS, GPA, MICROTOMOGRAPHY, DEVICE",

author = "J. Philippe and {Le Godec}, Y. and M. Mezouar and M. Berg and G. Bromiley and F. Bergame and Perrillat, {J. P.} and M. Alvarez-Murga and M. Morand and Robert Atwood and A. King and S. Regnier",

note = "Also funded by: 2. European Synchrotron Radiation Facility (ESRF) long-term project: HS2532 {"}Development of a new High P/T apparatus for X-ray studies{"}. Co-I Bromiley. (access supported through STFC) 3. DIAMOND UK light source, proposal EE9185 {"}Time resolved imaging of core formation in the early Earth: tomography at extreme conditions{"}. PI Bromiley (access supported through STFC). 4. NERC 0.5 studentship for Madeleine Berg (University of Edinburgh). 5. University of Edinburgh Principle's Career Development fund, 0.5 studentship for Madeleine Berg. ",

year = "2016",

doi = "10.1080/08957959.2016.1221951",

language = "English",

volume = "36",

pages = "512--532",

journal = "High Pressure Research",

issn = "0895-7959",

publisher = "Taylor & Francis",

number = "4",

}

Philippe, J, Le Godec, Y, Mezouar, M, Berg, M, Bromiley, G, Bergame, F, Perrillat, JP, Alvarez-Murga, M, Morand, M, Atwood, R, King, A & Regnier, S 2016, 'Rotating tomography Paris-Edinburgh cell: a novel portable press for micro-tomographic 4-D imaging at extreme pressure/temperature/stress conditions', High Pressure Research, vol. 36, no. 4, pp. 512-532. https://doi.org/10.1080/08957959.2016.1221951

TY - JOUR

T1 - Rotating tomography Paris-Edinburgh cell

T2 - a novel portable press for micro-tomographic 4-D imaging at extreme pressure/temperature/stress conditions

AU - Philippe, J.

AU - Le Godec, Y.

AU - Mezouar, M.

AU - Berg, M.

AU - Bromiley, G.

AU - Bergame, F.

AU - Perrillat, J. P.

AU - Alvarez-Murga, M.

AU - Morand, M.

AU - Atwood, Robert

AU - King, A.

AU - Regnier, S.

N1 - Also funded by: 2. European Synchrotron Radiation Facility (ESRF) long-term project: HS2532 "Development of a new High P/T apparatus for X-ray studies". Co-I Bromiley. (access supported through STFC) 3. DIAMOND UK light source, proposal EE9185 "Time resolved imaging of core formation in the early Earth: tomography at extreme conditions". PI Bromiley (access supported through STFC). 4. NERC 0.5 studentship for Madeleine Berg (University of Edinburgh). 5. University of Edinburgh Principle's Career Development fund, 0.5 studentship for Madeleine Berg.

PY - 2016

Y1 - 2016

N2 - This paper presents details of instrumental development to extend synchrotron X-ray microtomography techniques to in situ studies under static compression (high pressure), shear stress or the both conditions at simultaneous high temperatures. To achieve this, a new rotating tomography Paris-Edinburgh cell has been developed. This ultra-compact portable device easily and successfully adapted to various multi-modal synchrotron experimental set-up at ESRF, SOLEIL and DIAMOND is explained in detail. An in-depth description of proof of concept first experiments performed on a high resolution imaging beamline is then given, which illustrate the efficiency of the set-up and the data quality that can be obtained.

AB - This paper presents details of instrumental development to extend synchrotron X-ray microtomography techniques to in situ studies under static compression (high pressure), shear stress or the both conditions at simultaneous high temperatures. To achieve this, a new rotating tomography Paris-Edinburgh cell has been developed. This ultra-compact portable device easily and successfully adapted to various multi-modal synchrotron experimental set-up at ESRF, SOLEIL and DIAMOND is explained in detail. An in-depth description of proof of concept first experiments performed on a high resolution imaging beamline is then given, which illustrate the efficiency of the set-up and the data quality that can be obtained.

KW - High pressure

KW - high temperature

KW - tomography

KW - stress

KW - synchrotron

KW - NEUTRON POWDER DIFFRACTION

KW - IN-SITU

KW - COMPUTED-TOMOGRAPHY

KW - DEFORMATION

KW - TEMPERATURE

KW - APPARATUS

KW - GPA

KW - MICROTOMOGRAPHY

KW - DEVICE

U2 - 10.1080/08957959.2016.1221951

DO - 10.1080/08957959.2016.1221951

M3 - Article

SN - 0895-7959

VL - 36

SP - 512

EP - 532

JO - High Pressure Research

JF - High Pressure Research

IS - 4

ER -

Rotating tomography Paris-Edinburgh cell: a novel portable press for micro-tomographic 4-D imaging at extreme pressure/temperature/stress conditions

Abstract / Description of output

Keywords / Materials (for Non-textual outputs)

Access to Document

Fingerprint

Projects

In-Situ X-ray tomographic imaging under extreme conditions: a proof of concept study

Equipment

Electron Probe Microanalysis Facility (EPMA)

Micro CT Scanner (EXP)

Scanning Electron Microscope Facility (SEM)

Cite this