SHARPER-enhanced benchtop NMR: improving SNR by removing couplings and approaching natural linewidths

Claire L. Dickson; George Peat; Matheus Rossetto; Meghan E. Halse; Dusan Uhrin

doi:10.1039/D2CC01325H

SHARPER-enhanced benchtop NMR: improving SNR by removing couplings and approaching natural linewidths

Claire L. Dickson, George Peat, Matheus Rossetto, Meghan E. Halse, Dusan Uhrin

Research output: Contribution to journal › Article › peer-review

Abstract

We present a signal enhancement strategy for benchtop NMR that produces SNR increases on the order of 10 to 30 fold by collapsing the target resonance into an extremely narrow singlet. Importantly, the resultant signal is amenable to quantitative interpretation and therefore can be applied to analytical applications such as reaction monitoring.

Original language	English
Journal	Chemical Communications
Early online date	5 Apr 2022
DOIs	https://doi.org/10.1039/D2CC01325H
Publication status	E-pub ahead of print - 5 Apr 2022

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10.1039/D2CC01325H

20220422_Uhrin_d2cc01325h-VoRFinal published version, 1.87 MBLicence: Creative Commons: Attribution (CC-BY)

http://xlink.rsc.org/?DOI=D2CC01325H

SHARPER-enhanced benchtop NMR
Uhrin, D. (Creator) & Peat, G. (Creator), Edinburgh DataShare, 1 Sept 2022
DOI: 10.7488/ds/3439
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title = "SHARPER-enhanced benchtop NMR: improving SNR by removing couplings and approaching natural linewidths",

abstract = "We present a signal enhancement strategy for benchtop NMR that produces SNR increases on the order of 10 to 30 fold by collapsing the target resonance into an extremely narrow singlet. Importantly, the resultant signal is amenable to quantitative interpretation and therefore can be applied to analytical applications such as reaction monitoring.",

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AU - Dickson, Claire L.

AU - Peat, George

AU - Rossetto, Matheus

AU - Halse, Meghan E.

AU - Uhrin, Dusan

PY - 2022/4/5

Y1 - 2022/4/5

N2 - We present a signal enhancement strategy for benchtop NMR that produces SNR increases on the order of 10 to 30 fold by collapsing the target resonance into an extremely narrow singlet. Importantly, the resultant signal is amenable to quantitative interpretation and therefore can be applied to analytical applications such as reaction monitoring.

AB - We present a signal enhancement strategy for benchtop NMR that produces SNR increases on the order of 10 to 30 fold by collapsing the target resonance into an extremely narrow singlet. Importantly, the resultant signal is amenable to quantitative interpretation and therefore can be applied to analytical applications such as reaction monitoring.

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DO - 10.1039/D2CC01325H

M3 - Article

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JO - Chemical Communications

JF - Chemical Communications

ER -

SHARPER-enhanced benchtop NMR: improving SNR by removing couplings and approaching natural linewidths

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SHARPER-enhanced benchtop NMR

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